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ORDINANCE NO. 2012-007 IL Analytical Requirements. (1) The industrial user shall identify the pretreatment standards applicable to each regulated process. (2) In addition the industrial user shall submit the results of sampling and analysis identifying the nature and concentration (or mass where required by the pretreatment standard or control authority) of regulated pollutants in the discharge from each regulated process. Both daily maximum and average concentration (or mass where required) shall be reported. The sample shall be representative of daily operations In cases where the pretreatment standard requires compliance with a Best Management Practice or pollution prevention alternative the industrial user shall submit documentation as required by the control authority or the applicable standards to determine compliance with the standard. (3) The industrial user shall take a minimum of one representative sample to demonstrate data is in compliance with these requirements. (4) Samples shall be taken immediately downstream from pretreatment facilities, if such exist, or immediately downstream from the regulated process if no pretreatment exists. If other wastewaters are mixed with the regulated wastewater prior to pretreatment the industrial user shall measure the flows and concentrations necessary to allow use of the combined waste stream formula of subsection 62-625.410(6), FAC in order to evaluate compliance with the pretreatment standards. Where an alternate concentration or mass limit has been calculated in accordance with subsection 62-625.410(6), FAC this adjusted limit along with supporting data shall be submitted to the control authority. (5) All activities related to sampling and analysis shall comply with paragraphs (6)(d) and (e) and Chapter 62-160, F.A.C. ll Sampling activities shall be performed according to procedures specified in "The Department of Environmental Protection Standard Operating Procedures for Field Activities," DEP-SOP-001/01, March 31 2008 hereby adopted and incorporated by reference. A copy of this document is available for inspection at the FDEP's district offices and 2600 Blair Stone Road MS 3540, Tallahassee, Florida 32399- 2400 and is also available on the FDEP's internet site. (b) Analytical tests shall be performed in accordance with applicable test procedures identified in 40 CFR Part 136 as of July 1 2009 hereby adopted and incorporated by reference. If a test for a specific component is not listed in 40 CFR Part 136 or if the test procedure has been determined to be inappropriate for the analyte in question (e.g., insufficient sensitivity) the laboratory, with the approval of the industrial user and control authority, shall identify and propose a method for use in accordance with Rules 62-160.300 and 62-160.330, F.A.C. Coding: Words/letters/numbers underlined are additions to text; words/letters/numbers in *-i''*OUsT format are deletions to text. 30