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Indian River Farms WCD <br />7305 4th St. <br />Vero Beach,FL 32968 <br />FLUWILIPS INC. <br />P.O. Box 150597, Altamonte Springs, FL 32715-0597 Phone: 407-339-5984 E83018 (Mair. Lab) <br />571 NW Mercantile P1, Suite 111, Port St. Lucie, FL 34986 Phone: 772-343-8006 E86562 (South Lab) <br />812 SW Harvey Green Or, Madison, FL 32340 Phone: 850-973-6878 [82405 (North Lab) <br />3980 Overseas Hwy, Suite 103, Marathon, FL 33050 Phone: 305-743-8598 E35834 (Keys Lab) <br />PO #: n/a <br />Client Project #: Q -Canal Grabs <br />Date Sampled: Feb 4, 2016 <br />Feb 16, 2016; Invoice: 289668 <br />Lab,#`-:289668SW2; $ample`ii: �OTJU4'/.1610 4b`/A_M ti/D`e'sc: q�.Site#1 <br />.J =', ` ''t.� "e , <br />''kF7:a,,•�n,,,f b?;,. <br />r- •� .. <br /><^ r' -j <br />Parameter <br />_.- <br />Result <br />...iL - <br />Units <br />DF <br />MDL <br />c ,,!-> .,deAa>..?z` <br />PQL <br />QC Batch <br />Method <br />r.,c•..�,�',`:<r . <br />CAS # <br />,"t .,t :c;% <br />Analyzed <br />Surr:Bromofluorobenzene (50-170%) <br />100.77% <br />1.00 <br />1.00 <br />1.00 <br />10303283 <br />EPA8260 <br />460-004 <br />02/08/16 <br />Surr:Toluene-d8 (50-170%) <br />101.50% <br />1.00 <br />0.0100 <br />0.0100 <br />10303283 <br />EPA8260 <br />02/08/16 <br />Fecal Coliform <br />96.0 <br />cfu/100rrL <br />2.00 <br />2.00 <br />2.00 <br />10303332 <br />SM9222 D <br />E761792 <br />02/04/16 <br />12:15 PM <br />BOD5day <br />2.00 U <br />mg/L <br />1.00 <br />2.00 <br />2.00 <br />10303470 <br />SM5210 B <br />E1640606 <br />02/05/16 <br />12:00 PM <br />TKN(as N) <br />0.685-1 <br />mg/L <br />1.00 <br />0.200 <br />0.400 <br />10303519 <br />EPA351.2 <br />7727-37-9 <br />02/13/55 <br />Total Phosphorus(as P) <br />0.109 <br />mg/L <br />1.00 <br />0.0400 <br />0.100 <br />10303521 <br />EPA365.4 <br />7723-14-0 <br />02/13/55 <br />NO3+NO2(as N) <br />0.152' <br />mg/L <br />1.00 <br />0.0200 <br />0.0400 <br />10303888 <br />EPA353.2 <br />1-005 <br />02/15/16 <br />Ammonia (as N) <br />0.0708-/ <br />mg/L <br />1.00 <br />0.0100 <br />0.0200 <br />10303959 <br />EPA350.1 <br />7664-41-7 <br />02/15/16 <br />C:ab #:1489664SW3' "Samr"''leis:' 02/04/1.6'�1�I UOrAM;pp',`•Desc:n Site_#3�: ='�S ' `": � "� r Y �7 ' "�- ^- � I"" : '' <br />.P /,.., .,;:11. .. .. .. ..7- . .•. .�.1 !'A:t t' ,l. Sf1 L7'i7 {, l.l�rY:.y�C <br />•� : °`' '` `"' <br />i.:•f'T "-t i'y:i%1�.KSY.n`'t�i�,,�.�,,: .}:•W'-].,7ti�.:,�j•_.j.• <br />Parameter <br />Result <br />Units <br />DF <br />MDL <br />PQL <br />QC Batch <br />Method <br />CAS # <br />Analyzed <br />Turbidity <br />8.17 <br />NTU <br />1.00 <br />0.200 <br />0.400 <br />10276384 <br />EPA180.1 <br />G-019 <br />02/05/16 <br />02:30 PM <br />TSS <br />5.50/ <br />mg/L <br />1.00 <br />1.00 <br />2.00 <br />10303267 <br />SM2540 D <br />E1642818 <br />02/06/16 <br />Benzene <br />0.500 U <br />ug/L <br />1.00 <br />0.500 <br />1.00 <br />10303283 <br />EPA8260 <br />71-43-2 <br />02/08/16 <br />Ethylbenzene <br />0.500 U <br />ug/L <br />1.00 <br />0.500 <br />1.00 <br />10303283 <br />EPA8260 <br />100-41-4 <br />02/08/16 <br />Methyl-tert-butylether <br />1.00 U <br />ug/L <br />1.00 <br />1.00 <br />2.00 <br />10303283 <br />EPA8260 <br />1634-04-4 <br />02/08/16 <br />Toluene <br />0.500 U <br />ug/L <br />1.00 <br />0.500 <br />1.00 <br />10303283 <br />EPA8260 <br />108-88-3 <br />02/08/16 <br />Xylenes <br />1.00 U <br />ug/L <br />1.00 <br />1.00 <br />2.00 <br />10303283 <br />EPA8260 <br />1330-20-7 <br />02/08/16 <br />Surr:1,2-Dichloroethane-d4 (50-170%) <br />106.10% <br />1.00 <br />0.0100 <br />0.0100 <br />10303283 <br />EPA8260 <br />02/08/16 <br />Surr:Bromofluorobenzene (50-170%) <br />101.37% <br />1.00 <br />1.00 <br />1.00 <br />10303283 <br />EPA8260 <br />460-004 <br />02/08/16 <br />Surr:Toluene-d8 (50-170%) <br />101.83% <br />1.00 <br />0.0100 <br />0.0100 <br />10303283 <br />EPA8260 <br />02/08/16 <br />Fecal Coliform <br />120 B <br />cfu/100mL <br />2.00 <br />2.00 <br />2.00 <br />10303332 <br />SM9222 D <br />E761792 <br />02/04/16 <br />12:15 PM <br />BOD5day <br />2.00 LV <br />mg/L <br />1.00 <br />2.00 <br />2.00 <br />10303470 <br />SM5210 B <br />E1640606 <br />02/05/16 <br />12:00 PM <br />TKN(as N) <br />0.592- <br />mg/L <br />1.00 <br />0.200 <br />0.400 <br />10303519 <br />EPA351.2 <br />7727-37-9 <br />02/13/55 <br />Total Phosphorus(as P) <br />0.08461-/ <br />mg/L <br />1.00 <br />0.0400 <br />0.100 <br />10303521 <br />EPA365.4 <br />7723-14-0 <br />02/13/55 <br />NO3+NO2(as N) <br />0.175-1 <br />mg/L <br />1.00 <br />0.0200 <br />0.0400 <br />10303888 <br />EPA353.2 <br />1-005 <br />02/15/16 <br />Ammonia (as N) <br />0.03371 <br />mg/L <br />1.00 <br />0.0100 <br />0.0200 <br />10303959 <br />EPA350.1 <br />7664-41-7 <br />02/15/16 <br />FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) FLDOH: E35834 (Keys Lab) Page 3 of 7 <br />W <br />J <br />