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2017-142A
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Last modified
10/24/2017 4:26:20 PM
Creation date
10/10/2017 12:32:21 PM
Metadata
Fields
Template:
Official Documents
Official Document Type
Agreement
Approved Date
10/03/2017
Control Number
2017-142A
Agenda Item Number
8.I.
Entity Name
Department of Environmental Protection
Subject
Osprey Acres Stormwater Park
House Appropriations Grant
Water Quality Restoration Grant
Alternate Name
Osprey Acres Floway
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applicable. If requested by the Department, documentation that supports the DOC for a specified <br /> analyte and test method shall be made available for review. <br /> g. The contracted (and/or subcontracted) laboratory shall report PQLs and MDLs or other specified <br /> limits of detection and quantitation with the results of sample analyses. MDLs and/or PQLs shall <br /> only be required for test methods that are technically amenable to the determination of MDLs <br /> and/or PQLs. For those test methods where the determination of MDLs and/or PQLs are not <br /> technically feasible, the laboratory shall report a value or increment representing the lower limit of <br /> the working range of the test method, however determined by the laboratory. The laboratory shall <br /> indicate whether the reported limit represents a limit of detection or quantitation. In all cases, <br /> limits of detection and quantitation other than MDLs and PQLs shall be explicitly defined and <br /> evaluated by the laboratory. All limits shall be as listed in the applicable laboratory test method, <br /> SOP or Quality Manual, or as listed in the contract QA plan (Section 6, below). The reported <br /> MDLs and PQLs (or other limits per above) shall meet the analytical sensitivity and quantitation <br /> objectives for the contract. <br /> h. Additional laboratory quality control expectations: <br /> (i) The selected laboratory test methods listed in the QA Plan shall provide results that meet <br /> applicable contract data quality objectives. <br /> (ii) All laboratory testing procedures shall follow the analytical methods as approved in the <br /> contract QA plan(see Section 6). <br /> (iii) The laboratory shall adhere to the quality control requirements specified in the laboratory test <br /> methods and this Attachment. <br /> (iv)The laboratory shall calculate all sample results according to the procedures specified in the <br /> analytical test methods approved in the contract QA plan. <br /> 3. FIELD ACTIVITIES <br /> a. All sample collection and field testing activities shall be performed in accordance with the <br /> Department's "Standard Operating Procedures for Field Activities" (DEP-SOP-001/01, March 1, <br /> 2014). The specific standard operating procedures (SOPs) to be used for this contract shall be <br /> cited in the contract QA plan(see Section 6). <br /> b. Field-Generated Quality Control (QC) Blanks are defined in DEP SOP FQ 1000 (subparts FQ <br /> 1211 —FQ 1214)and shall be composed and analyzed for sample collection activities associated <br /> with this contract according to the requirements of part FQ 1230 (sections 1. —2.3.1), DEP SOP <br /> FS 2100(Part FS 2110, sec. 2.1.1.2) and/or DEP SOP FS 2400 (Part FS 2430, sec. 2.1.1.2), as <br /> applicable to the analytes and matrices to be collected using the sampling equipment specified in <br /> the contract QA plan (section 6 below). <br /> (i) If an analyte detected in the sample is also found in any field-generated QC blank that is <br /> associated with the sample, the contractor shall investigate and attempt to determine the <br /> cause of the QC blank contamination. If any contracted sample results are qualified as in(ii) <br /> below, the outcome of this investigation shall be reported to the DEP contract manager and <br /> shall include a discussion of the corrective measures taken to minimize future occurrences of <br /> QC blank contamination associated with the collection of samples for this contract. <br /> (ii) If an analyte detected in the sample is also found in any field-generated QC blank that is <br /> associated with the sample, the analytical result reported for the affected sample shall be <br /> qualified as an estimated value, unless the analyte concentration in the blank is less than or <br /> equal to 10% of the reported sample concentration. The "G" data qualifier code shall be <br /> reported with the sample result for any blank concentration exceeding the above "10%" <br /> criterion for the affected analyte(see Table 1, Chapter 62-160, F.A.C.). <br /> 4. REPORTING,DOCUMENTATION AND RECORDS RETENTION <br /> a. All laboratory and field records described or listed in Rules 62-160.240 and 62-160.340, F.A.C. <br /> shall be retained for a minimum of five years after the generation (or completion) of the records <br /> applicable to the contract. Longer retention times as specified in the contract shall supersede. <br /> b. All field and laboratory data and supporting information shall be reported for this contract <br /> according to applicable requirements in 62-160.340(3)through 62-160.340(8), F.A.C. <br /> Exhibit E,Page 2 of 6 <br /> DEP Quality Assurance Requirements for Contracts&Grants <br /> Standard Field&Lab Services <br /> Rev. 1-19-16 <br />
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